By Phil Danielson

 

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#1 - Pumpdown Curves as a Diagnostic Tool
Pumpdown curves can be a useful tool for diagnosing vacuum system problems. The collection, use, and interpretation of pumpdown curves are discussed and explained.   

Pumpdown Curves as a Diagnostic Tool  (.pdf file)

#2 - Rate-of-Rise Curves as a Diagnostic Tool
Rate-of-rise curves can be a powerful surveillance and diagnostic tool for vacuum problems. When used either alone or in consort with pumpdown curves, they can provide early warning of incipient vacuum problems and can help diagnose those problems. Interpretation and collection of the curves are discussed and explained.  [top of list]

Rate-of-Rise Curves as a Diagnostic Tool  (.pdf file)

#3 - Gas Loads from Elastomer and Metal Seals
Elastomer and metal gaskets are both in common use today. Each has its benefits and uses. An analysis of the mechanisms for gas loads from elastomer seals in terms of outgassing and atmospheric permeation is presented. Practical considerations and comparisons are provided to help make the elastomer vs. metal decision. 
[top of list]

Gas Loads from Elastomer and Metal Seals  (.pdf file)

#4 - Sorting Out the Turbo, Drag, and Turbo/Drag Pump Family
Turbomolecular, molecular drag, and turbo/drag pumps can be classified as a family. Although each type, within the family, is different, it is not always clear which is which when looking at manufacturers' literature. The difference is discussed and explained in terms of pumping mechanism, application, and roughing/backing requirements. 
[top of list]

Sorting Out the Turbo, Drag, and Turbo/Drag Pump Family  (.pdf file)

#5 - Knowing Your Effective Pumping Speed
The effective speed of a vacuum pump is the actual speed at the chamber. The importance of pumping speed in meeting gas loads is discussed. The effects of pumping speed losses through connecting tubulation in terms of conductance is shown. Simple methods for calculating both conductance and effective pumping speed are presented.  [top of list]

Knowing Your Effective Pumping Speed  (.pdf file)

 #6 - Dry Gas Techniques for Reducing Water Vapor in Vacuum Systems
The desorption of water vapor in vacuum systems is a constant and troublesome problem. The effects of desorption, evidenced by long pumpdown times, can be partially overcome by using various techniques involving dry gas in the chamber. The techniques and effects are explained and discussed. 
[top of list]

Dry Gas Techniques for Reducing Water Vapor in Vacuum Systems  (.pdf file)

#7 - The Difference Between Volume and Mass Flow
A certain amount of confusion exists in vacuum technology that can be traced to misunderstandings regarding the difference between volume and mass flow. The differences and their relative importance to the Q=SP relationship are discussed and explained. 
[top of list]

The Difference Between Volume and Mass Flow  (.pdf file)

 #8 - Understanding Virtual Leaks
The presence of virtual leaks can be a major problem in the performance of vacuum systems. Understanding what virtual leaks are and how they result in detrimental effects is discussed and presented. The practical techniques of eliminating them or minimizing their effects are given for both new designs and in existing systems. 
[top of list]

Understanding Virtual Leaks  (.pdf file)

#9 - Oil-Sealed Pumps and Backstreaming
Although there is a continuing trend toward replacing oil-sealed mechanical pumps with oil-free pumps, replacement is not always  necessary. In order to make a decision, it's necessary  to understand the source(s) and mechanisms of oil backstreaming from oil-sealed pumps. The sources and types of oil contamination are  explained and discussed along with techniques to eliminate or reduce backstreaming. 
[top of list]

Oil-Sealed Pumps and Backstreaming  (.pdf file)

#10 - Backstreaming Traps for Oil-Sealed Pumps
The use of traps to deal with the oil backstreaming from oil-sealed mechanical pumps can be dan acceptable solution or a potential disaster. In order to make the go/no go decision on their use, it is necessary to understand their trapping mechanisms along with what can go wrong if they are misunderstood or misused. Application advantages and penalties are discussed. 
[top of list]

Backstreaming Traps for Oil-Sealed Pumps  (.pdf file)

#11 - Recent Advances in Vacuum Sealing Techniques
Advances  in vacuum technology often proceed in  an  irregular fashion. Sealing techniques have been relatively static for some years, but new advances have recently been introduced to overcome the problems found with oil-rings. One is a metal seal that directly replaces ISO-KF/MF O-ring seals. Another is a totally gasketless sealing system. Their application is discussed. 
[top of list]

Recent Advances in Vacuum Sealing Techniques  (.pdf file)

#12 - The Vacuum Chamber: Volume or Surface Area?
Vacuum chambers are often configured during the design stage to keep the volume as low as possible. This consideration is usually applied under the assumption that this will reduce the gas load and result in faster
pumpdown. In fact, the surface area is the most important consideration. The source(s) of both surface and volume gas loads are discussed and explained. 
[top of list]

The Vacuum Chamber: Volume or Surface Area?  (.pdf file)

#13 - Crossover Pressure and Cryopumping
The crossover pressure from roughing pump to cryopump is often assumed to be as low a roughing pressure as possible in order to reduce the amount of gas condensed within the cryopump in the belief that this will extend the time between required regenerations. In fact, the maximum crossover pressure listed in the manufacturers' data sheets is actually the most ideal pressure. This concept is discussed and explained. 
[top of list]

Crossover Pressure and Cryopumping  (.pdf file)

#14 - Gas Loads and O-Rings
Careful consideration and understanding of gas loads from O-rings are important in understanding the behavior of vacuum systems. 
[top of list]

Gas Loads and O-Rings  (.pdf file)

#15 - Sources of Water Vapor in Vacuum Systems
Water vapor is a major problem in vacuum technology, but understanding its sources is a key to improving system performance. 
[top of list]

Sources of Water Vapor in Vacuum Systems  (.pdf file)

#16 - How To Assess Gas Loads in Vacuum System Design
A practical technique for assessing quantitative values for
gas loads. 
[top of list]

How To Assess Gas Loads in Vacuum System Desing  (.pdf file)

#17 - How To Choose a Diaphragm Pump
Understanding how diaphragm pumps work can help apply
them properly. 
[top of list]

How To Choose a Diaphragm Pump  (.pdf file)

#18 - How To Match Pumping Speed to Gas Load
Determining and understanding a vacuum system's gas loads and pumping speed will provide the key to designing or understanding the performance of any vacuum system. 
[top of list]

How To Match Pumping Speed to Gas Load  (.pdf file)

#19 - Gas Loads in Vacuum Systems
Using "gas load thinking" when considering vacuum problems streamlines the trouble-shooting process. 
[top of list]

Gas Loads in Vacuum Systems  (.pdf file)

#20 - Creating a Vacuum
What really happens within a vacuum chamber as it's pumped down to create a vacuum environment. 
[top of list]

Creating a Vacuum  (.pdf file)

#21 - Why Create a Vacuum?
Creating a vacuum  in terms of the physical and  chemical properties of a device or process. 
[top of list]

Why Create a Vacuum?  (.pdf file)

#22 - Desorbing Water in Vacuum System: Bakeout or UV?
Shorter pumpdown times or lower pressures can be achieved by using either bakout or UV energy to desorb water vapor. Here's how to make
the choice.  [top of list]

Desorbing Water in Vacuum System: Bakeout or UV?  (.pdf file)

#23 - How To Use Getters and Getter Pumps
Getter pumping can be an important addition to many vacuum processes if properly understood and applied. 
[top of list]

How To Use Getters and Getter Pumps  (.pdf file)

#24 - How To Use the Q=SP Fundamental Vacuum Relationship
Using and understanding vacuum technology's fundamental relationship
can be a vital and practical tool in applying vacuum technology to your process. 
[top of list]

How To Use the Q=SP Fundamental Vacuum Relationship  (.pdf file)

#25 - How To Choose a Roughing/Backing Pump for the Turbo and Drag Family
Choosing the right roughing/backing pump is as important as choosing the right high vacuum pump. The simple process of working through the pump's operating parameters will assure a successful installation. 
[top of list]

How To Choose a Roughing/Backing Pump for the Turbo and Drag Family  (.pdf file)

#26 - Contamination in Vacuum Systems: Sources and Remedies
Contamination can be scourge of any vacuum process. Learning how to detect and avoid contamination can lead to cleaner and more productive vacuum processes. 
[top of list]

Contamination in Vacuum Systems: Sources and Remedies  (.pdf file)

#27 - The Effects of Humidity on Vacuum System Performance
Humidity is the source of most of the water vapor problems encountered
in vacuum technology.  You can't fight a war unless you know your
enemy. 
[top of list]

The Effects of Humidity on Vacuum System Performance  (.pdf file)

#28 - Making the Oil-Sealed vs. Oil-Free Decision
Oil-free pumps can be a solution to oil contamination problems, but the decision to use them or not is complex. Working through the decision process requires a simple analysis of the options available. 
[top of list]

Making the Oil-Sealed vs. Oil-Free Decision  (.pdf file)

#29 - Molecular Flux Provides Process Understanding
Many process problems can be hidden when pressure is the only parameter monitored, but considering and understanding the flux of gas molecules through a process chamber can reveal effects that can make or break a process. 
[top of list]

Molecular Flux Provides Process Understanding  (.pdf file)

#30 - Vacuum Envelope Penetration
All vacuum systems are subject to penetration by atmospheric gases
due to leaks or permeation of the materials of construction. It is
important to understand the differences between these two different problems. 
[top of list]

Vacuum Envelope Penetration  (.pdf file)

#31 - Matching Vacuum Pump to Process
Choosing the best pump for a vacuum process can be a daunting
experience, but a systematic review of the process requirements and the performance parameters of the available pumps can help make the best choice. 
[top of list]

Matching Vacuum Pump to Process  (.pdf file)

#32 - Diagnosing Vacuum Problems with Pumpdown and Rate-of-Rise Curves
Pumpdown and rate-of-rise curves can provide simple tools to monitor and diagnose a system's performance and problems. 
[top of list]

Diagnosing Vacuum Problems with Pumpdown and Rate-of-Rise Curves  (.pdf file)

#33 - Pumping Water Vapor
Water vapor pumping presents problems to all vacuum processes, and pumping it requires careful understanding in order to achieve full pumpdown efficiency and performance.  [top of list]

Pumping Water Vapor  (.pdf file)

#34 - Vacuum Requirements for Cryogenic Vessels
Applying vacuum technology to cryogenic dewars and transfer
lines. 
[top of list]

Vacuum Requirements for Cryogenic Vessels  (.pdf file)

#35 - Understanding Pressure and Measurement
Pressure is an important component of the Q=SP fundamental vacuum relationship, but it means much more in practice and application.  [top of list]

Understanding Pressure and Measurement  (.pdf file)

#36 - Choosing the Right Vacuum Materials
An in-depth review of each and every material exposed to the vacuum system is absolutely essential to ensure a successful system design.  [top of list]

Choosing the Right Vacuum Materials  (.pdf file)

#37 - Will RGAs Replace Ion Gauges?
Pressure measurement in high vacuum can be important, but is an ion gauge good enough, or do you need a residual gas analyzer?  [top of list]

Will RGAs Replace Ion Gauges?  (.pdf file)

#38 - Solving Process Problems at the Molecular Flux Level
Working from pressure readings alone can mislead and misdirect a search for process problems, but reaching down a layer further into the molecular flux level can provide real solutions.  [top of list]

Solving Process Problems at the Molecular Flux Level  (.pdf file)

#39 - Matching Cryopumping Techniques to Application
Cryopumps and cryopumping have become fairly ubiquitous in vacuum technology. There are many variations within the category, and it is necessary to understand the variations in order to achieve the best practical results.  [top of list]

Matching Cryopumping Techniques to Application  (.pdf file)

#40 - Pumping Speed in the Drydown Zone
The extended pumpdown time through the water vapor-dominated drydown zone is a complex process that can be dissected to show that it is only partially dependent upon pumping speed.  [top of list]

Pumping Speed in the Drydown Zone  (.pdf file)

#41 - Bending the Rules: When the Vacuum Rules Get in the Way, Careful Analysis Allows Rule Bending

Vacuum technology has many fixed rules, but when the application requires the rules to be bent, careful analysis of the rules and application will often allow the rules to be worked around.  [top of list]

Bending the Rules (.pdf file)

#42 - The Use and Misuse of O-Rings

 Elastomer O-ring seals are commonly used to provide demountable vacuum seals. The proper choice of material, installation, and handling are key to a successful vacuum design.  [top of list]

The Use and Misuse of O-Rings (.pdf file)

#43 - Anatomy of a Pumpdown

Dividing a pumpdown curve into zones that reflect the actual gases being pumped within the zones is a useful technique for sorting out problems and solutions.  [top of list]

Anatomy of a Pumpdown (.pdf file)

#44 - Sealing Materials Require a Careful Choice

Elastomer and metal seals each have thier attendant advantages and disadvantages, but it is not always necessary to use either one exclusively. If the application is carefully considered, a mixed installation can be the best decision.  [top of list]

Sealing Materials Require a Careful Choice (.pdf file)

#45 - Thermal Conductivity Gauges

Thermal conductivity pressure gauges are extremely common in vacuum technology, but an understanding of their principles of measurement and operation can help in their proper application.  [top of list]

Thermal Conductivity Gauges (.pdf file)

#46 - Nitpicking Your Vacuum System

Detailed system analysis is a painful process that can make all the difference between a successful design or a total failure. It's all a question of mindset.  [top of list]

Nitpicking Your Vacuum System (.pdf file)

#47 – UV Conquers the Drydown Zone

All vacuum systems encounter the drydown zone where the slow desorption of water vapor controls the system’s pumpdown performance.  Powered desorption by UV radiation can shorten the pumpdown time substantially.  [top of list]

UV Conquers the Drydown Zone(.pdf file)

#48 –Understanding the Effects of Air Exposure

All vacuum systems are subject to the buildup of water vapor on surfaces during air exposure.  It’s now possible to quantify and compare the amount of water buildup under varying conditions of exposure.  [top of list]

Understanding the Effects of Air Exposure(.pdf file)

#49 – Pumpdown Effects of Water Vapor Buildup

The pumpdown performance in traversing the drydown zone can be quantified by calculating the monolayers of adsorbed water molecules and determining the subsequent desorption rate graphically.  [top of list]

Pumpdown Effects of Water Vapor Buildup(.pdf file)

#50 – Gas Purge Solutions to Oil and Water Contamination Problems

Contamination problems can be solved or avoided by special gas purging of the system and/or pumping lines during operation.  [top of list]

Gas Purge Solutions to Oil and Water Contamination Problems(.pdf file)

#51 – Pumping Specific Gases in High Vacuum

There’s more to planning and designing a vacuum process pumping system than just maximizing pumping speed.  Matching the pumping performance of each discrete gas species encountered will ensure maximum pumping performance.  [top of list]

Pumping Specific Gases in High Vacuum(.pdf file)

#52 – Conditioning  Vacuum Chambers

Confronting a high gas load from a new or newly cleaned vacuum chamber can be daunting, but there are some simple techniques for bringing it into normal condition.  [top of list]

Conditioning  Vacuum Chambers(.pdf file)

 

 

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Copyright © 2004 The Vacuum Lab
Last Modified:
November 07, 2006